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H. Nmrs, 1. , and C. , 250 MHz, CDCl3) ?= 9, pp.5-6

H. Nmr, CDCl3) ? 7, 20H, CHarom), 4.80 (h, J = 6.1 Hz, 1H, CH-(CH3)2), pp.3-6

C. Nmr, HRMS (ESI-MS): 746.1839 Da +/-1ppm IR (?, cm -1 , neat), 1887 (w) 1596 (w) (m) H NMR (250 MHz, CDCl3) ?= 7.58 (s, 1H, OH), pp.3018-2974

H. Nmr, CDCl3) ? 7, MHz, vol.664, issue.58, pp.37-44

H. Nmr, CDCl3) ? = 706 (s, 2H), 3, MHz, vol.5, issue.2, pp.6-6

R. Mhz, HRMS (ESI-MS): 762.1788 Da +-1 ppm IR (?, cm -1 , neat ) : 3317 (w,br), (m) H NMR (400 MHz, pp.2918-2862

R. Mhz, HRMS (ESI-MS): 762.1788 Da +/-1 ppm IR (?, cm -1 , neat ) : 3317 (w,br)(m), 701 cm -1 (m) Synthesispentakis(p-tolylthio)phenoxy)ethyl acrylate Alcohol 33 (1500 mg, 1.96 mmol), was dissolved in dry DCM (10 mL), Et3N (400 µL, 3.93 mmol) was added. The mixture was cooled to 0°C and acryloyl chloride (214 µL, 2.36 mmol) was added. The solution was warmed to room temperature and, The organic layer was dried over MgSO4 and filtered. After removal the solvent, the crude was purified by column chromatography over silica gel using cyclohexane/dichloromethane as eluent. Acrylate 31 was obtained as a yellow solid, pp.2918-2862

C. Nmr, HRMS (ESI-MS): 802.1737 Da +/-1 ppm IR (?, cm -1 , neat ) (m) cm -1 Synthesis of 38 (C35H32OS4): (2,3,5,6-tetrakis(p-tolylthio)phenyl)methanol Tetrafluorobenzyl alcohol (200 mg, 1.10 mmol), was dissolved in dry DMF (5 mL), K2CO3 (976 mg, 5.90 mmol) was added. The mixture was purged with Argon. The 4-methylbenzenethiol (823 mg, 5.60 mmol) was added. The reaction mixture was heated to 80 °C and stirred overnight, After reaction, the mixture was treated with NaOH 2M (50 mL) and extracted with CH2Cl2, pp.3018-2918

H. Nmr, CDCl3) ? 7, 1H), 5.08 (d, J = 7.2 Hz, 2H), 2.33 (s, 12H), pp.12-18

C. Nmr, HRMS (ESI-MS): 596.1336 Da+/-1ppm IR (?, cm -1 , neat ) : 3447 (w,br) (s) cm -1 Synthesis of 29 (C38H34O2S4): 2,3,5,6-tetrakis(p-tolylthio)benzyl acrylate Tetrasulfurated phenol (500 mg, 0.84 mmol), was dissolved in dry DCM (2 mL), Et3N (234 µL, 1.68 mmol) was added. The mixture was cooled to 0 °C and acryloyl chloride (81 µL, 1.01 mmol) was added. The solution was warmed to room temperature and stirred under Argon overnight. The organic phase was washed with H2O, MHz, vol.3020, issue.845, pp.2918-2855, 1920.

H. Nmr, 25 (s, 1H), 6.05 (dd, J = 17.2, 1.6 Hz, 1H) (s, 1H), MHz, vol.657, issue.2, pp.3-7

H. Nmr, CDCl3) ? 7, 12H), 6.75 (s, 2H), 4.98 (d, J = 6.6 Hz, 2H), 2.35 (s, 9H), 2.02 (t, J = 6.8 Hz, 1H), pp.23-29

H. Nmr, 72 (s, 2H), 6.35 (dd, J = 17.3, 1.5 Hz, 1H), 6.03 (dd, J = 17.3, 10.4 Hz, 1H), 5.77 (dd, J = 10.4, 1.5 Hz, 1H), 5.55 (s, 2H), pp.3-7

. Bromoiodobenzene, and phenylacetylene (450 mg, 4.40 mmol) were stirred for 6 h with CuI (76.0 mg, 0.40 mmol) of and Pd(PPh3)4 as catalysts (231 mg, 0.40 mmol) in 5 mL of piperidine at 0 °C. The reaction mixture was acidified with HCl 2M, and 30 mL of CH2Cl2 was added. The organic phase was washed twice with HCl 2 M and H2O. After removal the solvent, the crude was purified by column chromatography over silica gel using cyclohexane/dichloromethane as eluent

H. Nmr, CDCl3) ? 7, MHz, vol.7, pp.72-79

C. Kubel, S. L. Chen, and K. Mullen, Poly(4 '-Vinylhexaphenylbenzene)s: New Carbon-Rich Polymers Synthesis of 46 (C42H29Br): (4-Bromophenyl)pentaphenylbenzene Compound 44 (700 mg, 2.74 mmol) of and tetracyclone 45 (1.20 g, 3.15 mmol) were heated to 250 °C in 3 mL of diphenyl ether during 94 h. The raw product was washed with 20 mL of cold n-hexane and recrystallized from toluene, Macromolecules, issue.18, pp.31-6014, 1998.

H. Nmr, CDCl3) ? 7.20 (d, J = 8.5 Hz, MHz, vol.7, issue.6, pp.15-21

C. Kubel, S. L. Chen, K. Mullen, and . Poly, Vinylhexaphenylbenzene)s: New Carbon-Rich Polymers Synthesis of 47 (C44H32): 4-Vinylhexaphenylbenzene Compound 46 (1410 mg, 2.00 mmol) and tributylvinylstannane (698 mg, 2.20 mmol) were reacted in dry toluene 40 mL with Pd(PPh3)4 (46 mg, 0.04 mmol) and 2,6-di-tert-butyl-4-methylphenol 5 mg to prevent polymerization. The solution was heated to reflux for 6 h. After reaction, Macromolecules, issue.18, pp.31-6014, 1998.

C. Kubel, S. L. Chen, K. Mullen, and . Poly, -Vinylhexaphenylbenzene)s: New Carbon-Rich Polymers Synthesis of 51 (C16H14O4S2): 4,4'-Dithiobisbenzoic acid dimethyl ester 4, Dithiobisbenzoic acid was heated at reflux in MeOH (100 mL) with H2SO4 conc, pp.31-6014, 1998.
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C. Nmr, 101 MHz, CDCl3) ? 167

H. Nmr, DMSO-d6) ? 7, MHz, vol.74, issue.709